GH133合金高温低周疲劳研究
High Temperature Low Cycle Fatigue of GH133 Superalloy
-
摘要: 本文研究了GH133合金的循环应力应变反应和低周疲劳性能,并作了位错结构和断口观察。通过对比拉压对称(R=-1)试验和恒定最大正应变(εmax=C)试验,证明平均拉应力起降低寿命的作用。位错结构观察证明,循环使共格γ′质点的相界处产生应力场,最终导致位错的萌生并运动,位错运动又进一步增殖位错。位错运动方式是变化的,由成对切割γ′质点到单位错切割γ′质点和位错绕过γ′质点。滑移带位错结构最终可以出现饱和的梯状结构,与典型的驻留带位错结构相似。晶界和双晶界附近位错密度高,具有位错胞结构,同时可以出现沿晶界裂纹和沿双晶界裂纹。
在循环交变作用下,材料的破坏过程可以分解为三个主要过程,即在循环作用下产生的材料变形行为的变化,疲劳裂纹的形成和疲劳裂纹不断扩展,直到一定的临界大小而发生最终破坏,这三个过程是不同的但又是相互联系的,宏观疲劳现象可以在此基础上作出适当的说明。对于含有共格γ′沉淀相的低层错能奥氏体合金,许多研究1—8指出,其循环反应往往是先循环硬化再循环软化,并具有面排列位错结构。关于循环软化现象,一些作者认为8,共格沉淀相在位错往复切割下碎化而导致回溶,...Abstract: The cyclic stress-strain responce and microstructures(TEM) were studied in LCF samples of 15Cr-27Ni-1.8Ti-Fe alloy. The strain control LCF tests were performed at 600* under two different wave mode:R=-1 and fixed eeeemax. Comparing the results of these two kind tests, the detrimantal effect of average tensile stress was proved. This was comcerned with the influenceof tensile stress on the movement of dislocations and the fromation ocracks.
The observations of dislocations structure indicated that during the cycling both mechanisms causing cyclic hardening and cyclic softening were taking place. Cyclic strain led to generate the stress-field at the interface of γ and γ' phases first. As a result of increasing stress field the dislocations were created.The density of dislocation was further increased by the move, ment of dislocations themself. The interactions between dislocations and γ particles degenerated from pair dislocation cutting γ' particles to single dislocation cutting γ'particles. It led to form more faults and APB'S, and the γ' particles became propressively harder to shear and ultimately led to dislocations looping around particles.
A typical dislocation structure of persistant slip hand, laddie-like stracture was seen asasatureted dislocation structure in the slip band,and the more laddie-like structure formed, the more cyclic softening happened.
The slip band extended to grain boundaries and twin boundaries, The grain diclocations interacted with boundaries, and led to complex boundary dislocations structure the density of dislocations near grain boundaries andtwin boundaries was much higher than others since the boundaries can actedas the barrier and dislocation generator. This would cause to form grainboundary cracks and twin boundary cracks.