真空液相重结晶法改善InSb薄膜的组织和性能

Improving Structure and Electrical Properties of InSb Films by Vacuum Recrystallization

  • 摘要: 利用真空下氩气保护液相重结晶的方法,对热蒸镀和磁控贱射制得的Insb薄膜进行热处理.X射线衍射和组织分析的结果表明:热处理前薄膜为Insb,In,Sb各相的混合物;重结晶后,基本为InSb单相,InSb晶粒呈规则状外形长大.热处理后室温下的电子迁移率大大提高,由原来的1.31×104 cm2/(V·s)提高到4.47×104 cm2/(V·s)(热蒸镀)和2.15×103 cm2/(V·s)提高到2.04×104 cm2/(V·s)(磁控溅射).

     

    Abstract: A heat-treatmentprocedure has been applied to InSb films prepared by thermal evaporation and magnetron sputtering, the films have been recrystallised from the melt in the vaccum with Ar protection.From the X-ray diffraction and SEM structure studies, it is found that the InSb films are mixtures of InSb, In, Sb before heat treatmentand are mainly single phase of InSb after recrystallization. The InSb grains grow with faceted interface and regular morphology. Theelectron mobility of InSb films (at room temperature) have been increased greatly after heat-treatment with 1.31×104 cm2 /(V·s) to 4.4×104 cm2 /(V·s) (thermal evaporation) and 2.15×103 cm2/(V·s) to 2.04×104 cm2/(V·s) (magnetron sputtering) respectively.

     

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