定向凝固过程中的流动效应

Convective effects during unidirectional solidification

  • 摘要: 在类合金(NH4Cl-H2O溶液)定向凝固晶体生长实验装置上,利用ϕ30μm煤粉作示踪粒子,再现糊状区内微通道流以及通道出口处的流体流动,并测算了各处流体的瞬时速率.分析认为:凝固初期,糊状区内固相体积分数较大,内部流体流动受阻;随着固相体积分数减少,糊状区孔隙率增大,流体充分发展;当平均固相体积分数降至0.42,接近最小值0.38时,当量雷诺数达到临界值(247),糊状区内形成微通道;随着通道宽度逐渐扩大,液相区内热流体进入微通道.微通道内稀冷液体向上流,浓热液体向下流,促使通道内溶液再结晶.

     

    Abstract: Directional solidification experiments were carried out using the analogue casting system of NH4Cl-H2O solution by cooling it from below. The transient velocities of fluid flow within the micro-channel of mushy layer were measured by using observation facility and tracer coal particles of 30 μm in diameter. It turned out that during the solidification process, the mean solid fraction of mushy layer descended rapidly at first, so the mushy layer got more permeable and natural convection was more likely to occur. When the mean solid fraction was down to 0.42, and closed to the smallest value of 0.38, and the equivalent Reynolds number exceeded the critical value, about 247, plume convection with associated micro-channel occurred in the mush. With the expanding of channel width, the solution of liquid region, whose temperature was higher than that of mushy layer, flowed into the micro-channel. The convection within the channel was found to consist of upward flow and downward flow. The counter flow advected heat away and solute which was favorable to solidification, so that solution within the channel recrystallized.

     

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